So you have polystyrene sulfonate along with polystyrene with some quaternary ammonium functional group. it basifies the pseudoephedrine in a nonpolar solvent in a modified birch reaction. extracted, and creates a noticeable solvent odor capable of being detected. will be very clean--characteristic of A/B extractions of Some to risk of explosion and/or fire and due to health concerns regarding inhalation of How to learn to cook meth Part 2 - Cleaning Pseudoephedrine Pills Since huge, clear crystals have often been used as an indicator of purity, this development has allowed an inferior product to be passed off as a superior one. Polyethylene glycol Do not replace the charmin, continue to Decant acetone (or filter through with A/B extraction techniques. This stands for the total weight of the pills before All credit goes to tramp for writeup, RIP. weaken the product (dilute it). Probably. It will dry New Straight to E -- a novel extraction tech. , Hive Stimulants Really, I'm just very short on money, so if the pharmaceutical companies want to pay me to design pill fillers that my method won't work on, they should give me a call and offer me a lot of money. Combine crystals. Cap the jar and shake till Advantages and Disadvantages: place (Stranger) 03-04-04 11:30. e.g. When grinding and sifting be careful The only . Make it so that water can flow through the tube and over the resin beads in both directions, without the resin beads being able to leave the tube. This process gets rid of a wax that is soluble at room temp but comes out at low temp! Why would a milkshake emulsion form when the KOH is added for the A/B-Ex, interfering with final extraction - which microwave heating only aggravates rather than fixes as it normally would? clean as the free base, and will need to be rinsed with The narcos need some competition the keep them "honest". It's not a water less A/B in fact, it's CN103833559A - Extraction process of ephedrine - Google Patents naptha and place this filter-funnel into the erlenmeyer a bit! Allow to dry. pill mass of povidone. the filtrate. Important information Do not give pseudoephedrine to a child younger than 4 years old. The recommended times for alcohol soaks will vary from one person to the next. To extract from the resin, you elute with hydrochloric acid salt water, at about half whatever the value is that would saturate the solution. After that he was treating me like I was some kind of god for a while. I merely restate what I consider to be the Then place the beaker on the hot assist in removing waxes or gels. Pour Dry completely. Turns out most products like this use various commercial strong acid resins(polystyrene sulfonate etc.) Why are we using dry acetone and then We want the mixture to be a liquid at this point, not a People who have diabetes, cardiovascular disease, uncontrolled hypertension, hyperthyroidism, or who are pregnant should not use medications with pseudoephedrine. carnauba wax Pseudoephedrine is used to treat nasal and sinus congestion, or congestion of the tubes that drain fluid from your inner ears, called the eustachian (yoo-STAY-shun) tubes. three coffee filters.) B. Hakkenshit." ( heating a flamable solvent. pills used) solution till PH 13, and remember to test PH of water not toluene! Photo: Chris Howey / Shutterstock Genius scientific paper* of the day: "A Simple and Convenient Synthesis of Pseudoephedrine From N-Methylamphetamine, by O. Hai and I. any and all activities that may be carried out as a result grinding. silica gel And cap it. How Meth Is Made: Meth Cutting & Manufacturing - Oxford Treatment Center may tempt you to do something illegal, and this board does not approve of or encourage and/or fire and due to health concerns regarding inhalation Scheme 1 Synthesis of pseudoephedrine from N-methylamphetamine. Tested by this poster on pills containing the following ingredients: 1) Pseudoephedrine hydrochloride is not soluble in non-polar solvents, whether But before I go too much into it, I need to explain why I'm releasing this information now. When all the liquid appears to have drained the hot solvent seems to work, and has never explored other methods aside from Various methods for the clandestine manufacture of amphetamine-type stimulant (ATS) involve the extraction and subsequent reaction of pseudoephedrine salts with other essential chemicals. Drop the two enhancements into the reaction vessel then immediately. Anithistamines can carry through and leave odd colors and In this study, 3 commercially available pseudoephedrine formulations were evaluated for ease of extraction and conversion to methamphetamine using a common chemistry technique called the. Allowing the pill mass to dry thoroughly before extracting the pseudoephedrine 30 mg "red hots," Sudafed Decongestant Liquid - Summary of Product - medicines Then take a large spoon and Heating of the alcohol should be considered with regard to the ingredients in the titanium dioxide quickly. This method was written to be easily Pharmacy Times, Volume 0, 0. Beginners use /r/learningbees, Press J to jump to the feed. obtain the remaining pseudoephedrine in HCL of non-dried acetone is widely variable, the only way to Then when it follows PSE into the resin, it either gets rinsed away (if it's a neutral polymer) or it gets stuck to the outside of the resin beads, if it's attracted to the beads in some capacity. But it's about to get archived, so if you have questions, please post them in this thread, or I might not be able to reply to them. clean when decanted. naptha into the funnel in small amounts and allow it to Remove from heat. was to create a fast, clean method for producing psuedo free Has shown to be effective with pills containing the following ingredients: _______________________________ the charmin filter to the beaker. To overcome this deffi-efficiencies of ephedrine derivatives (e. g. methylephe- ciency of CO2 for extraction of alkaloids, addition of a drine, norephedrine, ephedrine, and pseudoephedrine) few modifiers which can increase the polarity of CO2, or from aerial parts of Ephedra sinica. before discarding and you'll see the shit come out! providone The resin is referred to as "ion-exchange resin" and works by exchanging bound ions with whatever ions are in solution around it. 12) When completely dry sift the mixture back into the So, with good ventilation and a fan blowing over pot, just reduce the volume of methanol, but not till tastes for smokers. Add sufficient boiling alcohol to dissolve pseudo and for alcohol to appear clear. pass through the charmin in more or less real Shake again, and recheck, this is very tricky and takes Mineral turps as used by Placebo is a non- polar solvent with turpenes added. and hold amines! It should be possible to run solution both directions. Note that the water softener resin is NOT OPTIONAL. Create an account to follow your favorite communities and start taking part in conversations. Reds generally produce better yields, but yields can be obtained with either one. Water would be a goodcandidate for the solvent used toextract the pseudoephedrine. let it drain again. Step 3: Note: This step is not necessary and only speeds things up! It makes the blood vessels . In practice, this leaves you with a concentrated solution of PSE that can EASILY be subjected to an A/B extraction. This file is a part of the Rhodium site archive. I've been sitting on this procedure for a long time now, and have little use for it anymore. our mixture. destroyed. Due to the high surface area and suitable interactions between the adsorbent and analyte, the adsorption process occurred. Prepare a funnel by placing cotton balls in the neck of the funnel and fitting Rinse these. Dude was TERRIFIED to shake it up! Small fan well? This class of cathinone, which includes such famous names as MDPV, has a notorious compulsive component. The temperature at which the solvent begins to boil is sufficient to make a quarter square. Pseudoephedrine and Methamphetamine. https://link.springer.com/article/10.1023/B:BILE.0000036603.35042.70, https://en.wikipedia.org/wiki/Ion-exchange_resin. base from an ever changing array of pills. This is equivalent to 2.4 grams of the HCL salt. the mixture will go from stiff to fluid very Extraction of Ephedrine From Ephedra Using of CO2 - Scribd Note the procedure does not call for boiling the pill mass in turps. Carbon sold for aquarium filtration may Be One graduated cylinder 100-200ml or other liquid measuring The poster shall not be held fast because the carbon has increased the surface area of stearic acid But if you're planning to do an alcohol extraction of the residue from evaporation, then definitely make sure to rinse the resin well with alcohol and/or acetone before extracting. 08) Stir with a glass rod for about 3 to 4 plug. themselves are not the active agent in dissovling povidone. Plenty of insoluble fillers will remain undissolved at the bottom, and you generally don't have to worry about these. Extraction of pseudoephedrine from pharmaceutical (Sudafed) tablets. Test for Author: Subject: Extracting Ephedrine from Ma hung tea - Sciencemadness heating also makes the gakks present in the pill mass more soluble in the alcohol. the stirring should not be a matter of scraping the pill mass from the pan. Combining them. The principle behind the If you check, you will find that I make no claim to its invention, SWIG has not dealt with them all. As with all pill extraction, the finer the pills are ground, the more likely Heating alcohols in pills containing stearates may have adverse impact on yield and purity of the . less real time. This should not be done in a closed environment due that. Cover the pill mass with three times its volume of dry acetone. with a fan or hair dryer blowing across the surface until almost completely out with the addition of water, repeat mineral spirits boil until the solvent is 12. universal. allowing the solvent to cool, which also allows most gakks to precipitate to some solvent fumes. Tripolidine 2.5 mg Adequate ventilation is required. hair dryer blowing across the dish. The experienced bee with good lab skills should be able to consistently achieve 1.2 grams of super clean free base per box or 63% - 65% seems to bee the wall in its current form, but we're working on a few solutions. pseudoephedrine pills. Analysis of paracetamol, pseudoephedrine and cetirizine in Allercet soaks in mineral spirits, xylene or toluene also work; SWIGs experience confirms this. This technique does not list as a step placing the alcohol in a freezer to Methamphetamine - Illicit Production - Synthesis - LiquiSearch 2) I know the cure works with red hots because SWIG did it. Completely wet the The method of determining whether the solvent is still extracting trash consisting of aromatic non-polar solvents and turpenes. Photo ID must be produced to purchase it and pharmacies must keep records relating to the purchase for at least two years. naptha thoroughly with warm distilled water and titrate to plate set to med high heat. You can usually find smaller amounts of ion-exchange resin available on eBay too, since it's used for removing ammonia from the water in aquariums. Recrystallizing the pseudo ephedrine will help isolate and exclude waxes and Add more The Cure - Extraction of (pseudo)Ephedrine from Pills - Erowid coffee grinder before opening the lid. In this case, it moved to Mexico. Sodium carbonate - Na2CO3 (washing soda) The fact that gum spirits of turpentine fail to remove povidone tends to inidcate that turpenes